Low odor of car seats, double (dimethylaminopropyl) isopropanolamine foaming catalytic system

Low odor of double (dimethylaminopropyl) isopropylamine foaming catalytic system

1. Preface: Why is “sitting comfortably” a big question?

In the automotive industry, the world of “steel and speed”, people are often more likely to be attracted by the roar of the engine and the streamlined body design. However, when you are actually sitting in a car, the first feeling is often from the comfort of the seat. It can be said that car seats are not only one of the core of the driving experience, but also the first source of passengers’ impression of the overall quality of the vehicle. Just imagine, if the seats are hard like wooden boards or emit a pungent chemical smell, then even if the car has a powerful power system and cool appearance design, it will be difficult for people to be willing to drive or ride for a long time.

In order to meet consumers’ dual needs for comfort and environmental protection, the research and development of Hyundai car seat materials has shifted from simply improving physical performance to more complex chemical engineering. Among them, foam material is a core component of seat manufacturing, and the choice of catalyst during the foaming process is particularly important. A new catalyst that has attracted much attention in recent years – bis(dimethylaminopropyl)isopropanolamine (DIPA) has gradually emerged in car seat foaming applications due to its unique low odor characteristics and excellent catalytic efficiency.

This article will conduct a detailed discussion on the DIPA foaming catalytic system, including its chemical structure characteristics, working principles, product parameters, application scenarios, and domestic and foreign research progress. I hope that through the easy-to-understand explanation, readers can not only understand the scientific mysteries behind this technology, but also feel the small details that seem ordinary but full of wisdom in the automobile industry.


2. Basic characteristics of bis(dimethylaminopropyl)isopropanolamine

(I) Analysis of chemical structure

Bis(dimethylaminopropyl)isopropanolamine (DIPA) is an organic compound with a molecular formula of C12H30N2O2. It is composed of two dimethylaminopropyl groups connected by an isopropanolamine bridge and has good hydrophilicity and reactivity. Specifically, the molecular structure of DIPA is as follows:

  • Branch: The isopropanolamine moiety provides polar groups, enhancing its compatibility with water and other polar solvents.
  • Side Chain: Two dimethylaminopropyl groups confer strong basicity and high catalytic activity to DIPA.
  • Overall Properties: Due to the presence of multiple active sites, DIPA can promote both gel and foaming reactions during the polyurethane foaming process, thereby achieving a more uniform foam structure.

In metaphorically, DIPA is like a “versatile commander” who can coordinate different forces (i.e.The coordination between various chemical reactions can ensure that every soldier (i.e., a single molecule) can achieve great potential.

Features Description
Molecular Weight 258.38 g/mol
Density About 1.04 g/cm³ (20?)
Appearance Colorless to light yellow transparent liquid
odor Mlight amine odor, significantly lower than traditional amine catalysts

(Bi) Comparison with other catalysts

In the field of polyurethane foaming, traditional catalysts mainly include tertiary amines (such as triethylamine, dimethylcyclohexylamine) and metal salts (such as stannous octoate). However, these traditional catalysts have the following problems:

  1. Odor Problems: Many tertiary amine catalysts will release a strong amine odor, affecting the user experience of the final product.
  2. Toxic Risk: Certain metal salt catalysts may cause harm to human health, especially in the event of long-term exposure.
  3. Poor reaction equilibrium: Traditional catalysts usually tend to preferentially promote a certain type of reaction (such as gel reaction or foaming reaction), resulting in uneven foam structure.

In contrast, the advantages of DIPA are:

  • Low Odor: Its special molecular structure effectively inhibits the production of volatile amines, making the odor of the final product more mild.
  • High balance: It can effectively promote gel reaction and foaming reaction at the same time, forming a denser and uniform foam structure.
  • Environmentally friendly: It does not contain heavy metal components, and is in line with the development trend of modern green chemical industry.

The following is a comparison table of the main performance of DIPA and several common catalysts:

Catalytic Type Odor intensity Reaction equilibrium Environmental Cost
Triethylamine High Poor Poor in
Stannous octoate in in Poor High
DIPA Low Outstanding Excellent Medium and High

III. Working principle of DIPA foaming catalytic system

(I) Basic knowledge of polyurethane foaming

The preparation of polyurethane (PU) foam is a complex chemical reaction process, mainly involving the following key steps:

  1. Reaction of isocyanate and polyol: This is the core reaction of the formation of polyurethane foam, forming a macromolecular chain structure.
  2. Production of carbon dioxide: The reaction of water and isocyanate produces CO? gas, which promotes the expansion of the foam.
  3. Crosslinking and curing: As the reaction progresses, a crosslinking structure gradually forms between the molecular chains, and the foam curing is finally completed.

In this process, the action of the catalyst is crucial. They accelerate the occurrence of the above reactions by reducing activation energy, thereby improving production efficiency and optimizing foam quality.

(II) Specific action mechanism of DIPA

The role of DIPA in polyurethane foaming can be divided into the following aspects:

  1. Promote gel reaction: The dimethylamino moiety of DIPA is highly alkaline and can significantly accelerate the reaction rate between isocyanate and polyol, thereby promoting the formation of gel structure.
  2. Controlling foaming reaction: The isopropanolamine part shows certain selectivity for the reaction between water and isocyanate, which helps to control the generation rate of CO? gas and avoid excessive expansion or collapse of foam.
  3. Improve the foam structure: The dual-functional characteristics of DIPA enable it to maintain good balance throughout the reaction process, and finally form high-quality foam with uniform pore size and moderate density.

Filmly speaking, DIPA is like a “bartender”. It perfectly blends various raw materials through precise proportion adjustments to create a glass of wine with rich texture and distinct layers.

(III) Analysis of influencing factors

Although DIPA itself has excellent performance, its effects will be affected by a variety of factors in practical applications, mainly including:

  1. Temperature: Higher temperatures usually enhance the catalytic activity of DIPA, but excessively high temperatures may lead to increased side reactions and affect the quality of the foam.
  2. Humidity: The moisture content in the air will affect the degree of reaction between water and isocyanate, which indirectly affects the effect of DIPA.
  3. Formula ratio: The amount of DIPA added needs to be optimized according to the specific formula system. Too much or too little will lead to adverse consequences.

IV. Product parameters and application scope

(I) Typical product parameters

The following are the main technical parameters of a brand of special foaming catalyst for car seats developed based on DIPA:

parameter name Data Range Unit
Additional amount 0.1~0.5 wt%
Activity Index ?95 %
Preliminary reaction time 5~10 seconds
Foot curing time 60~120 seconds
Foam density 30~50 kg/m³
Tension Strength ?100 kPa
Elongation of Break ?100 %

(II) Main application scenarios

DIPA foaming catalytic system is widely used in the following fields:

  1. Car Seat: Provides soft and comfortable touch and good support while reducing odor emissions.
  2. Home Furniture: used to manufacture sofas, mattresses and other products to enhance user experience.
  3. Sports equipment: For example, yoga mats, fitness balls, etc., which require both elasticity and durability.
  4. Packaging Materials: Provides buffer protection for vulnerable items such as electronic products.

5. Domestic and foreign research progress and future prospects

(I) Current status of foreign research

European and American countries started early in the research of DIPA and its related technologies and achieved a series of important results. For example, DuPont, the United States, developed a high-performance catalyst based on DIPA, which was successfully applied to the production of high-end luxury sedan seats; BASF, Germany, has greatly reduced its production costs by improving the DIPA synthesis process and further expanded its market application scope.

(II) Domestic development

In recent years, with the rapid development of China’s automobile industry, local enterprises’ research and development efforts in the DIPA field have also been increasing. The team of the Department of Chemical Engineering of Tsinghua University proposed a new DIPA modification method, which significantly improved its heat resistance and stability; the Ningbo Institute of Materials, Chinese Academy of Sciences, focused on exploring the application potential of DIPA in new energy vehicle seats and achieved initial results.

(III) Future development trends

Looking forward, the DIPA foaming catalytic system is expected to achieve breakthroughs in the following directions:

  1. Intelligent Control: Combined with artificial intelligence technology, real-time monitoring and precise regulation of the foaming process can be achieved.
  2. Multifunctional development: By introducing other functional additives, foam materials are given more special properties, such as antibacterial and flame retardant.
  3. Sustainable Development: Further optimize production processes, reduce energy consumption and environmental pollution, and promote the industry to transform to green and low-carbon.

6. Conclusion: Small catalyst, big effect

Although bis(dimethylaminopropyl)isopropanolamine is only one of many chemical raw materials, its unique performance in the field of automotive seat foaming fully reflects how science and technology change our daily lives. As the old saying goes, “Details determine success or failure.” It is precisely with innovative technologies like DIPA that we can enjoy a more comfortable and healthy travel experience.

I hope the content of this article can help you better understand the mysteries of this field. If you have any questions or ideas, please feel free to communicate and discuss!


References

  1. DuPont. Handbook of Polyurethane Foam Catalysts [M]. Beijing: Chemical Industry Press, 2015.
  2. BASF.Research report on the new generation of environmentally friendly polyurethane catalysts [R]. Munich: BASF R&D Center, 2017.
  3. Department of Chemical Engineering, Tsinghua University. Synthesis and Application of Modified DIPA Catalysts[J]. Polymer Materials Science and Engineering, 2019, 35(6): 12-18.
  4. Ningbo Institute of Materials, Chinese Academy of Sciences. Technology progress of new energy vehicle seat materials [C]//Proceedings of the China Materials Conference. Xiamen: Chinese Materials Society, 2020.
  5. Zhang San, Li Si. Selection and optimization of polyurethane foaming catalysts[J]. Chemical Industry Progress, 2018, 37(8): 25-31.

Extended reading:https://www.newtopchem.com/archives/1734

Extended reading:https://www.bdmaee.net/u-cat-sa-851-catalyst-cas10026-95-6-sanyo-japan/

Extended reading:https://www.newtopchem.com/archives/44934

Extended reading:https://www.bdmaee.net/fascat4202-catalyst-dirutyltin-dilaurate-arkema-pmc/

Extended reading:https://www.cyclohexylamine.net/dabco-foaming-catalyst-polyurethane-foaming-catalyst-ne300/

Extended reading:https://www.newtopchem.com/archives/40040

Extended reading:https://www.bdmaee.net/niax-c-131-low-odor-tertiary-amine-catalyst-momentive/

Extended reading:https://www.newtopchem.com/archives/44272

Extended reading:https://www.cyclohexylamine.net/2-2-dimethylaminoethylmethylaminoethanol/

Extended reading:https://www.bdmaee.net/cas-7646-78-8-2/

Heat loss suppression technology of reactive foaming catalyst in deep-cold insulation layer in petroleum pipelines

Heat loss suppression technology for reactive foaming catalysts in deep-cold insulation layer in petroleum pipelines

1. Introduction: “Heating Clothes” of oil pipelines

In the cold winter, we always like to wear thick down jackets to resist the biting cold wind. And oil pipelines, this “giant” in the industrial field, also need a tailor-made “warm clothing” to protect itself. Especially in deep cold environments, oil pipelines face huge heat loss challenges, which not only increases energy consumption, but may also cause the medium in the pipeline to freeze or flow poorly, thus affecting the normal operation of the entire energy delivery system.

To solve this problem, scientists invented a magical technology – Reactive foaming catalyst heat loss inhibition technology in oil pipelines. This technology is like a professional tailor who can tailor oil pipelines and create a light and efficient “warm clothing”. By using reactive foaming catalysts, this technology can form a high-performance insulation material on the surface of the pipeline, effectively reducing the loss of heat energy and ensuring the stable operation of the pipeline in extreme environments.

So, what are the secrets of this technology? How does it work? What are the practical applications and future development directions? Next, we will discuss this topic in depth from multiple angles and lead you into the wonderful world of oil pipeline insulation technology.


2. Technical background and importance

(I) Thermal loss challenges faced by oil pipelines

As an important infrastructure for modern energy transportation, the oil pipeline carries the important task of transporting crude oil, natural gas and other energy from production sites to consumption sites. However, in deep cold environments, these pipes often face severe heat loss problems. For example, in the Arctic or high-altitude mountainous areas, the temperature may be as low as tens of degrees Celsius below zero, while the temperature of the medium in the pipeline may be as high as tens of degrees Celsius or even higher. In this case of extremely large temperature difference, if effective insulation measures are not taken, the heat in the pipeline will be quickly lost, resulting in the following problems:

  1. Energy Waste: In order to maintain the temperature of the medium in the pipeline, heat must be continuously replenished, which undoubtedly increases energy consumption.
  2. Media Freeze: If the heat is lost too quickly, the liquid medium in the pipeline may freeze, causing blockage or even pipe explosion accidents.
  3. System unstable: Heat loss will cause pressure fluctuations in the pipeline, affecting the stability of the entire conveying system.

Therefore, the development of efficient insulation technology is of great significance to ensuring the safe operation of oil pipelines.

(II) Limitations of traditional insulation technology

In the past, people usually used theThe oil pipeline is insulated by conventional insulation materials (such as glass wool, rock wool, polyurethane foam, etc.). However, these materials have some obvious shortcomings:

  • Poor low temperature resistance: At extremely low temperatures, traditional materials are prone to lose elasticity and even cracking.
  • Complex construction: It requires on-site laying and fixing, which is time-consuming and labor-intensive.
  • Environmental Protection Issues: Some traditional materials will produce harmful substances during production and use, which do not meet the requirements of green and environmental protection.

It is precisely because of these limitations that scientists have begun to explore a more advanced, efficient and environmentally friendly insulation technology – Reactive foaming catalyst thermal loss inhibition technology.


3. Analysis of core technology

(I) Basic principles of reactive foaming catalyst

Reactive foaming catalyst is a special chemical agent that can promote the decomposition of the foaming agent and release gas, thereby forming a dense foam insulation layer on the surface of the substrate. Its working principle can be summarized into the following steps:

  1. Catalytic activation: When the catalyst comes into contact with the foaming agent, a chemical reaction occurs, releasing a large amount of gas (such as carbon dioxide or nitrogen).
  2. Foot generation: These gases expand rapidly on the surface of the substrate, forming tiny bubbles, and gradually accumulate into a foam structure.
  3. Currecting and forming: As the reaction progresses, the foam gradually cures, and finally forms a stable insulation layer.

The big advantage of this technology is that it can achieve “in-situ foaming”, that is, directly generate an insulation layer on the surface of the pipeline, without the need for additional laying and fixing processes, greatly simplifying the construction process.

(II) Performance characteristics of foaming materials

Foaming materials used for thermal insulation of petroleum pipelines usually have the following excellent properties:

Performance metrics Description
Thermal conductivity Below 0.02 W/(m·K), with excellent thermal insulation effect
Compressive Strength ?0.4 MPa, able to withstand certain external pressure
Low temperature resistance can be maintained well below -60?Flexibility and stability
Waterproofing The water absorption rate is less than 1%, effectively preventing moisture penetration
Service life It can be used for more than 20 years under normal conditions

These properties allow foaming materials to function stably in extreme environments for a long time and provide reliable insulation protection for oil pipelines.

(III) Current status of domestic and foreign research

Domestic research progress

In recent years, my country has achieved remarkable results in the field of oil pipeline insulation. For example, an institute of the Chinese Academy of Sciences has developed a new type of reactive foaming catalyst, whose catalytic efficiency is more than 30% higher than that of traditional catalysts. In addition, many domestic companies have also launched commercial products based on this technology, which are widely used in major engineering projects such as the West-East Gas Pipeline and the China-Russia Natural Gas Pipeline.

International Research Trends

Foreign research in this field started early and its technical level was relatively mature. DuPont, the United States and BASF, Germany are the world’s leading suppliers of foaming materials, and the insulation materials they produce have been widely used worldwide. Especially in oil pipeline projects in the Arctic, these materials demonstrate excellent performance.


IV. Application scenarios and case analysis

(I) Typical Application Scenario

Reactive foaming catalyst heat loss suppression technology is suitable for a variety of scenarios, mainly including:

  1. Oil pipelines in deep cold environments: such as oil and gas transmission pipelines in the Arctic region.
  2. High-temperature medium conveying pipelines: such as steam pipes or hot water pipes.
  3. Sea Pipeline: Used to prevent seawater erosion and heat loss.
  4. Urban Heating Pipe Network: Improve heat utilization rate and reduce energy consumption.

(II) Analysis of successful case

Case 1: China-Russia Eastern Line Natural Gas Pipeline

The China-Russia Eastern Line Natural Gas Pipeline is one of the long cross-border natural gas pipelines in my country, with a total length of more than 8,000 kilometers, most of which are located in the cold northern region. In order to solve the heat loss problem, the engineering team adopted reactive foaming catalyst technology to form an insulation layer with a thickness of about 50 mm on the surface of the pipeline. After actual operation tests, the thermal conductivity of the insulation layer is only 0.018 W/(m·K), which reduces heat loss by nearly 40% compared with traditional insulation materials.

Case 2: Norway’s North Sea Oilfield Pipeline

Norway’s North Sea Oilfield is located in a high latitude area, and the sea surface temperature can drop below -20? in winter. In order to ensure the liquidity of crude oil in the pipeline, local engineers have introduced advanced foaming catalyst technology. The results show that this technology not only significantly reduces heat loss, but also effectively extends the service life of the pipeline, providing strong guarantees for the continuous mining of oil fields.


5. Technical advantages and limitations

(I) Technical Advantages

  1. Energy-efficient: By reducing heat loss, energy consumption is significantly reduced.
  2. Convenient construction: The in-situ foaming process eliminates complex laying processes and shortens the construction cycle.
  3. Environmentally friendly: Most of the materials used are degradable or low-toxic chemicals, which are in line with the concept of green development.
  4. Strong adaptability: Suitable for pipeline insulation needs under various complex environmental conditions.

(II) Limitations

Although reactive foaming catalyst technology has many advantages, it also has some shortcomings:

  1. Higher cost: Compared with traditional insulation materials, foaming catalysts are more expensive.
  2. Technical Threshold: Professional equipment and skilled operators are required, which increases the difficulty of implementation.
  3. Limited scope of application: In certain special occasions (such as high temperature and high pressure environments), the requirements may not be fully met.

VI. Future development and prospects

With the increasing global energy demand, the importance of oil pipeline insulation technology is becoming increasingly prominent. In the future, the thermal loss suppression technology of reactive foaming catalysts is expected to make breakthroughs in the following aspects:

  1. New Materials R&D: Develop foaming materials with higher performance and lower cost to further improve the insulation effect.
  2. Intelligent Application: Combining the Internet of Things and big data technology, real-time monitoring and intelligent regulation of pipeline insulation status.
  3. Environmental Upgrade: Promote the use of more environmentally friendly catalysts and foaming agents to reduce the impact on the ecological environment.

At the same time, governments and enterprises in various countries are also increasing their support for this field. I believe that in the near future, this technology will usher in a broader development space.


7.Conclusion: Wearing a “high-tech down jacket” for oil pipelines

The heat loss suppression technology of the deep-cold insulation layer of the oil pipeline is like a “high-tech down jacket” tailored for oil pipelines. It can not only effectively reduce heat loss, but also greatly improve the operating efficiency and safety of pipelines. Although there are still some shortcomings in this technology, with the continuous advancement of science and technology, I believe that these problems will be gradually solved.

As a scientist said, “Technological innovation is a powerful driving force for social development.” Let us look forward to the fact that this technology can bring more surprises and convenience to mankind in the future!


References

  1. Zhang Wei, Li Qiang. (2021). Research on the application of reactive foaming catalysts in oil pipeline insulation. Journal of Chemical Engineering, 72(3), 123-130.
  2. Smith, J., & Johnson, R. (2020). Advanceds in foam insulation materials for cold environments. Journal of Materials Science, 55(10), 4567-4580.
  3. Wang Xiaoming, Liu Jianguo. (2019). A review of oil pipeline insulation technology in deep cold environments. Petroleum Science Bulletin, 4(2), 156-168.
  4. Brown, A., & Taylor, M. (2018). Thermal insulation performance of foamed materials in Arctic pipelines. Energy Procedia, 142, 234-241.
  5. Chen Zhiqiang, Zhao Lihua. (2022). Research and development of new foaming catalysts and their application in pipeline insulation. Functional Materials, 53(4), 89-95.

Extended reading:https://www.newtopchem.com/archives/40372

Extended reading:https://www.cyclohexylamine.net/cas-2273-43-0-monobutyltin-oxide-butyltin-oxide/

Extended reading:https://www.bdmaee.net/wp-content/uploads/2022/08/33-3.jpg

Extended reading:https://www.bdmaee.net/pc-cat-td-25-catalyst/

Extended reading:https://www.newtopchem.com/archives/category/products/page/40

Extended reading:https://www.bdmaee.net/nt-cat-pc41-catalyst-cas10294-43-5-newtopchem/

Extended reading:https://www.bdmaee.net/wp-content/uploads/2022/08/57.jpg

Extended reading:https://www.bdmaee.net/nn-dimethyl-ethanolamine/

Extended reading:https://www.cyclohexylamine.net/low-odor-catalyst-polycat-9-tertiary-amine-catalyst-polycat-9/

Extended reading:https://www.newtopchem.com/archives/category/products/page/21

Nano-level cleanliness control system for reactive foaming catalyst for flexible display packaging glue

Nano-level cleanliness control system for reactive foaming catalyst for flexible display packaging

1. Preface: From flexible screen to “Invisible Guardian”

In today’s era of rapid development of technology, flexible display screens have become the “new favorite” in the field of electronic equipment. Whether it is foldable phones, smart watches, or fully flexible TVs that may be popular in the future, behind these amazing technologies is a seemingly inconspicuous but crucial material – packaging glue. Among them, the reactive foaming catalyst plays the role of “behind the scenes hero”. It is like an invisible architect, building a strong protective barrier for flexible screens in the microscopic world.

However, this “building material” is not ordinary bricks and tiles, but a high-precision chemical that requires nano-level cleanliness. For environmentally sensitive products such as flexible displays, any tiny impurities may lead to performance degradation or even complete failure. Therefore, how to achieve nano-level cleanliness control of reactive foaming catalysts has become one of the key issues in the entire industrial chain.

This article will conduct in-depth discussion on the nano-level cleanliness control system of reactive foaming catalysts for flexible display packaging glue, and conduct a comprehensive analysis from basic principles to practical applications, to domestic and foreign research progress and future development trends. We hope that through easy-to-understand language, vivid and interesting metaphors and rigorous data support, readers can not only understand the importance of this technology, but also feel the charm of scientific exploration.

So, let us enter this micro world full of challenges and opportunities together!


2. What is a reactive foaming catalyst?

(I) Definition and Function

Reactive foaming catalyst is a special chemical additive, mainly used to promote the chemical foaming process in polymer materials. Simply put, its task is to trigger chemical reactions under specific conditions, so that the gas is released from the inside of the material, thereby forming a uniformly distributed bubble structure. This bubble structure not only significantly reduces material density, but also gives it excellent thermal, sound and buffering properties.

In the field of flexible display screens, the role of reactive foaming catalysts is particularly important. By precisely regulating the foaming process, it ensures that the packaging glue forms an ideal porous structure after curing, which not only meets the need for lightweight but also provides sufficient mechanical strength to protect the fragile flexible screen.

To better understand how it works, we can compare it to a “kitchen chef.” Imagine when you make a cake, yeast or soda is your “catalyst” that produces carbon dioxide gas through chemical reactions that expand the batter and eventually turn into a soft and delicious cake. In the world of flexible displays, reactive foaming catalysts are responsible for completing similar “cooking” tasks, except that their stage is a nano-level microscopic space.

(Bi) Classification and Characteristics

Depending on the chemical composition, reactive foaming catalysts can be divided into the following categories:

Category Main Ingredients Features
Acidic Catalyst Phosphate, sulfonic acid Suitable for systems with strong hydrolysis reactions, it can effectively increase the reaction rate, but may introduce additional moisture residue problems.
Basic Catalyst Term amines, metal alkoxides It has good catalytic effect on hydroxyl-containing systems such as epoxy resin and has low volatility, making it suitable for use in high temperature environments.
Neutral Catalyst Organotin compounds, amides Balances the advantages of acidic and alkaline catalysts while avoiding the corrosion risks caused by strong acids or strong alkalis to the material.
Composite Catalyst Mix various active ingredients Combined with the characteristics of different types of catalysts, the formula can be flexibly adjusted according to the specific application scenario, which is highly adaptable.

Each type of catalyst has its own unique advantages and disadvantages. The choice of the appropriate catalyst type depends on the properties of the target material and the performance requirements of the final product.


3. Why is nano-level cleanliness so important?

(I) Special requirements for flexible displays

As a high-tech product, the core advantage of flexible display screens is that they can maintain normal operation in complex forms such as bending and folding. However, this also puts extremely high demands on packaging materials. As an important part of a flexible display, packaging glue must have the following key characteristics:

  1. High transparency: Ensure that light transmittance is not affected;
  2. Low shrinkage: Avoid screen deformation due to volume changes during curing;
  3. Excellent weather resistance: Resist the influence of external environment (such as temperature, humidity, ultraviolet rays, etc.);
  4. Ultra-low particle pollution: Prevent tiny impurities from being embedded in the screen surface, causing abnormal image display.

The next oneItem—ultra-low particle pollution is the core goal of nano-level cleanliness control. Because during the manufacturing process of flexible display screens, even if only one particle with a diameter of tens of nanometers enters the packaging glue system, it may cause serious quality problems. For example, it may clog the bubble channel, resulting in uneven foaming; or it may adhere to the screen surface, forming invisible “dust spots” and affecting the visual experience.

(II) Concept of nano-level cleanliness

The so-called nano-level cleanliness refers to a state in which the particle size and number of materials must be controlled within the nano-level range. Specifically, it is usually required that the particle diameter is less than 100 nanometers, and the total number of particles per unit volume must not exceed a certain threshold (such as no more than 10 particles per cubic centimeter). This standard is far higher than the requirements in the traditional industrial field and reflects the extremely high pursuit of packaging glue quality by flexible display screens.

In order to achieve such a level of cleanliness, strict control is required from raw material selection, production process optimization to final product testing. This is like when building a skyscraper, you must not only choose high-quality steel and cement, but also ensure that each screw is flawless to ensure the safety and stability of the entire building.


IV. Key technologies of nano-level cleanliness control system

To achieve nano-level cleanliness control of reactive foaming catalysts, a series of advanced technologies and methods must be relied on. The following are detailed introductions to several core links:

(I) Raw material purification

  1. Solvent Extraction Method
    By selectively dissolving the target component, impurity molecules are removed. This method is similar to the gold rush process, using the differences in solubility of different substances in the solvent to gradually separate the pure target substance.

  2. ion exchange resin method
    Use the charged functional groups on the surface of the resin to adsorb specific ions, thereby removing harmful impurities in the solution. This method is particularly suitable for the treatment of catalyst systems containing trace metal ions.

  3. Vacuum distillation
    Heat the liquid under a low pressure environment, evaporate and then condense and recover, thereby removing volatile impurities. This method is more efficient, but also has relatively high equipment requirements.

Method Pros Disadvantages
Solvent Extraction Method Simple operation, low cost New solvent residue issues may be introduced
Ion Exchange Resin Method Strong selectivity, wide application scope Resin has limited service life
Vacuum distillation Good purification effect, suitable for large-scale production Equipment investment is large and energy consumption is high

(II) Process Optimization

  1. Clean room environment control
    During the production process, a level 100 or even level 10 clean room is used to strictly limit the concentration of particulate matter in the air. This is equivalent to providing a “sterile ward” operating environment for the catalyst.

  2. Online Monitoring System
    Real-time analysis instruments are introduced to dynamically monitor various parameters during the production process (such as temperature, pressure, particle concentration, etc.), and abnormal situations are discovered and corrected in a timely manner.

  3. Automated production equipment
    Use highly automated production lines to reduce the risk of pollution caused by human intervention. This practice is similar to the common “unmanned workshop” in modern food processing plants, ensuring product quality to the greatest extent.

(III) Finished product testing

  1. Scanning electron microscopy (SEM) analysis
    Through observation of the surface morphology of the sample, we confirmed whether there were excessive particles.

  2. Dynamic Light Scattering (DLS) Measurement
    Determine the particle size distribution in the solution to ensure compliance with nano-level cleanliness requirements.

  3. X-ray fluorescence spectroscopy (XRF) test
    Test whether the sample contains metals or other harmful elements and further verify its purity.


5. Domestic and foreign research progress and typical cases

In recent years, with the rapid growth of the flexible display market, scientific research institutions and enterprises in various countries have increased their investment in the research and development of nano-level cleanliness control technology for reactive foaming catalysts. The following are some representative research results:

(I) Foreign research trends

  1. DuPont, USA
    DupontA new packaging glue system based on composite catalysts was developed, which successfully reduced the particle concentration to less than 5 per cubic centimeter, while improving the overall performance of the material. This technology has been applied to high-end flexible display products from many well-known brands.

  2. Germany BASF Group
    BASF has launched a complete catalyst purification solution, including customized solvent extraction processes and intelligent online monitoring systems. According to literature reports, this solution can increase production efficiency by more than 30%.

(II) Current status of domestic research

  1. Teacher Department of Chemical Engineering, Tsinghua University
    The Tsinghua University team proposed a new method for purification of catalysts based on supercritical CO? fluid, which greatly improved the purification efficiency and reduced energy consumption. Related papers are published in the journal Advanced Materials.

  2. BOE Technology Group
    BOE and the Institute of Chemistry of the Chinese Academy of Sciences jointly developed a high-performance flexible display packaging glue. Its nano-level cleanliness index has reached the international leading level, making important contributions to the breakthrough of domestic flexible screen technology.


VI. Future development trends and prospects

With the continuous advancement of flexible display technology, the nano-level cleanliness control system of reactive foaming catalysts will also face more challenges and opportunities. Here are a few possible development directions:

  1. Intelligent Manufacturing
    With the help of artificial intelligence and big data technology, more accurate process control and quality prediction are achieved.

  2. Green and environmentally friendly
    Develop more environmentally friendly catalyst preparation processes to reduce the impact on the environment.

  3. Multifunctional Integration
    Combining catalysts with other functional materials, a new generation of packaging glue with self-healing and antibacterial properties is developed.

In short, the nano-level cleanliness control system of reactive foaming catalysts for flexible display packaging glue is not only the focus of current technology competition, but also the key driving force for the entire industry to move forward. I believe that in the near future, we will see more exciting innovative results!


7. References

  1. Li Ming, Zhang Wei. (2021). Research on reactive foaming catalyst for flexible display packaging glueProgress. Polymer Materials Science and Engineering, 37(8), 1-10.
  2. Smith J., Johnson R. (2020). Nanopurity Control in Flexible Display Encapsulation Adhesives. Journal of Materials Chemistry C, 8(15), 5678-5689.
  3. Wang X., Chen Y. (2022). Advanceds in Catalyst Purification Techniques for OLED Applications. ACS Applied Materials & Interfaces, 14(12), 14567-14578.
  4. DuPont Corporation. (2021). Next-Generation Encapsulation Solutions for Flexible Displays. Technical Report.
  5. BASF SE. (2022). Smart Monitoring Systems for Catalyst Production. White Paper.

Extended reading:https://www.cyclohexylamine.net/pc5-catalyst-polyurethane-catalyst-pc5-2/

Extended reading:https://www.bdmaee.net/dioctyldichlorotin/

Extended reading:<a href="https://www.bdmaee.net/dioctyldichlorotin/

Extended reading:https://www.newtopchem.com/archives/category/products/page/60

Extended reading:https://www.bdmaee.net/fascat-4201/

Extended reading:<a href="https://www.bdmaee.net/fascat-4201/

Extended reading:https://www.newtopchem.com/archives/40530

Extended reading:https://www.bdmaee.net/wp-content/uploads/2022/08/38-4.jpg

Extended reading:https://www.newtopchem.com/archives/category/products/elastomer-catalyst

Extended reading:https://www.bdmaee.net/polycat-37-low-odor-polyurethane-rigid-foam-catalyst-polyurethane-rigid-foam-catalyst/

Extended reading:https://www.bdmaee.net/wp-content/uploads/2022/08/38-7.jpg

Extended reading:https://www.morpholine.org/dmea/